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A hydroformylation process for the preparation of heterocyclic derivatives (by machine translation)
A hydroformylation heterocyclic derivatives of the preparation method, the invention relates to a hydroformylation heterocyclic derivatives of the preparation method. The purpose of this invention is to solve the formylation heterocyclic derivative synthesis required for high-temperature heating system, high energy consumption, conditions are harsh requirement to the equipment is large, but also the problem of low yield, the invention at room temperature, the heterocyclic derivatives, 2, 2 – ethoxy acetic acid, oxidizing agent and alkali may be dissolved in the organic solvent, mix, then nitrogen 25 – 35 min, then placed under the blue LEDs lamp illumination reaction is complete, then the acid catalytic hydrolysis, adjusting the pH to neutral, and then by silica gel column chromatography separation and purification, can be obtained by formylation of heterocyclic derivatives. The method of the invention under normal temperature and can be reaction, mild reaction conditions, yield can be up to 80%, and has a simple operation, pollution-free, safety and environmental protection, the advantage of low cost. The invention is applied to the field of organic synthesis. (by machine translation)
Note that a catalyst decreases the activation energy for both the forward and the reverse reactions and hence accelerates both the forward and the reverse reactions.Safety of 5-Chloroisoquinoline, you can also check out more blogs about5430-45-5
Reference：
Isoquinoline – Wikipedia,
Isoquinoline | C9H1537N – PubChem