82827-09-6,82827-09-6, 6-Bromoisoquinolin-1(2H)-one is a isoquinoline compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
6-bromoisoquinoline-1 (2Eta)-one (12 mmol), bis(3,5-dichlorophenyl)disulfide (10 mmol), six in sequence in a pressure-resistant reaction tube at room temperature Silver fluoride (10 mmol) and dichloroethane (8 mL). The reaction mixture was then reacted at 90 C for 10 hours. The reaction was quenched and concentrated under reduced pressure to give a crude material which was washed with a mixture of petroleum ether and ethyl acetate. Fast column chromatography to obtain the corresponding product 4-(3,5-Dichlorophenylthio)-6-bromoisoquinoline-1 (2H)-one. Yield 75%;
The synthetic route of 82827-09-6 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Nankai University; Zhu Youquan; He Jingli; Niu Yunxia; Han Tingfeng; Li Haoyu; (14 pag.)CN108822035; (2018); A;,
Isoquinoline – Wikipedia
Isoquinoline | C9H7N – PubChem