147497-32-3, 6-Bromo-3,4-dihydroisoquinolin-1(2H)-one is a isoquinoline compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Step 1 Preparation of 6-bromo-1,2,3,4-tetrahydroisoquinoline A solution of 6-bromo-3,4-dihydro-1(1H)-isoquinolinone (Example 31, Step 1; 5.5 g, 1.0 mmol) in THF (25 mL) was treated with 1M BH3 in THF (5 mL, 5 mmol) and heated at reflux for 20 h. To the mixture was added MeOH (5 mL), the solvent removed and the residue heated with 2N HCl for 3 h. The reaction was cooled, made basic with aqueous NH4 OH and extracted with CH2 Cl2, dried and evaporated to give the title compound as a gum which was used as such., 147497-32-3
The synthetic route of 147497-32-3 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Merck & Co., Inc.; US5977134; (1999); A;,
Isoquinoline – Wikipedia
Isoquinoline | C9H7N – PubChem