22246-12-4, 6-Methoxy-3,4-dihydroisoquinolin-1(2H)-one is a isoquinoline compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
The compound 27-1 (250 mg, 1.41 mmol) was dissolved in DMF (10 mL), and in ice bath, added with NaH (84 mg, 2.11 mmol, 60%), after reacting for 10 min, the mixture was dripped with iodomethane (300 mg, 2.11 mmol) and warmed slowly to room temperature, then further reacted for 2 hours. LCMS monitored the completion of the reaction, the reaction solution was extracted by adding saturated saline solution and ethyl acetate. The organic phase was washed twice by saturated saline solution. The organic phases were combined, dried and concentrated to dryness, to afford the brown liquid product 27-2 (225 mg, 83%)., 22246-12-4
As the paragraph descriping shows that 22246-12-4 is playing an increasingly important role.
Reference£º
Patent; Sichuan Kelun-Biotech Biopharmaceutical Co., Ltd.; ZHU, Jiawang; SONG, Zhiquan; YANG, Long; LI, Rui; ZHANG, Shuai; ZHOU, Lin; ZHAO, Mingliang; TANG, Zujian; ZHONG, Wei; ZENG, Hong; SONG, Hongmei; ZHOU, Xin; TAN, Yuting; HU, Xiao; WANG, Lichun; WANG, Jingyi; (99 pag.)EP3617186; (2020); A1;,
Isoquinoline – Wikipedia
Isoquinoline | C9H7N – PubChem