82827-09-6, 6-Bromoisoquinolin-1(2H)-one is a isoquinoline compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
82827-09-6, Example 25 6-Bromo-4-chloroisoquinolin-1(2H)-one 6-Bromoisoquinolone (300 mg) was dissolved in N,N-dimethylacetamide (7.0 mL), NCS (215 mg) was added to the solution and the mixture was stirred at 50 C. for 50 minutes. Water was added to the reaction liquid, the insoluble material precipitated out of the liquid was collected by filtration and then washed with isopropyl alcohol to give a desired product (245 mg) as yellow powder. 1H NMR (CDCl3, 400 MHz): delta 7.56 (1H, d, J=6.1 Hz), 7.78 (1H, dd, J=8.6, 1.8 Hz), 7.92 (1H, d, J=1.8 Hz), 8.14 (1H, d, J=8.6 Hz), 11.72 (1H, s). ESIMS (+): 258 [M+H]+.
The synthetic route of 82827-09-6 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Kohno, Yasushi; Sumiya, Tatsunobu; Takita, Satoshi; Kojima, Akihiko; US2011/178041; (2011); A1;,
Isoquinoline – Wikipedia
Isoquinoline | C9H7N – PubChem