Archives for Chemistry Experiments of Isoquinoline-4-carbaldehyde

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Treatment of heteroaryl-aldehydes with diethyl cyanophosphonate in the presence of a catalytic amount of LiCN affords phosphorylated cyanohydrins which are reduced in situ with SmI2 to give heteroaryl-acetonitriles in generally good overall yields (50-100%). The generality of the process is demonstrated.

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Reference：
Isoquinoline – Wikipedia,
Isoquinoline | C9H7N – PubChem